版權(quán)說明:本文檔由用戶提供并上傳,收益歸屬內(nèi)容提供方,若內(nèi)容存在侵權(quán),請進(jìn)行舉報或認(rèn)領(lǐng)
文檔簡介
1、Designation:D4745?14StardClassificationSystemBasisfSpecificationfFilledPolytetrafluoethlyene(PTFE)MoldingExtrusionMaterialsUsingASTMMethods1ThisstardisissuedunderthefixeddesignationD4745thenumberimmediatelyfollowingthede
2、signationindicatestheyearofiginaladoptioninthecaseofrevisiontheyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperepsilon()indicatesaneditialchangesincethelastrevisionreapproval.1.Scope1.1Thiss
3、tardclassificationsystembasisfspecificationcoverspolytetrafluoethylene(PTFE)filledmoldingcompoundsmadewithvirginPTFEresinsdefinedinSpecificationD4894asTypesIIIII.NOTE1—ThissystemcanbeusedasamodelfotherPTFEcompoundshaving
4、particulatefillersthatcansurvivethesinteringtemperaturesofPTFEascanthoselistedinthisstard.ThissystemisrestrictedtovirginPTFEbaseresinftechnicalreasons.Recycledreprocessedmaterialcannotbeprocessedsuccessfully.NOTE2—Thepro
5、pertiesmeasuredoncommerciallyfabricatedpartsmaydifferfromthelistedvaluesfsamplespreparedbytheproceduresgiveninthisspecificationdependingonpartgeometryprocessingparameters.1.2ThevaluesstatedinSIunitsaretoberegardedasstard
6、.1.3ThefollowingstatementappliestothetestmethodptionSection11ofthisspecification:Thisstarddoesnotpurpttoaddressallofthesafetyconcernsifanyassociatedwithitsuse.Itistheresponsibilityoftheuserofthisstardtoestablishappropria
7、tesafetyhealthpracticesdeterminetheapplicabilityofregulatylimitationspritouse.SeeNote5faspecificwarningstatement.NOTE3—ThereisnoknownISOequivalenttothisstard.2.ReferencedDocuments2.1ASTMStards:2D792TestMethodsfDensitySpe
8、cificGravity(RelativeDensity)ofPlasticsbyDisplacementD883TerminologyRelatingtoPlasticsD1600TerminologyfAbbreviatedTermsRelatingtoPlasticsD1708TestMethodfTensilePropertiesofPlasticsbyUseofMicrotensileSpecimensD3892Practic
9、efPackagingPackingofPlasticsD4894SpecificationfPolytetrafluoethylene(PTFE)GranularMoldingRamExtrusionMaterialsIEEEASTMSI10StardfUseoftheInternationalSystemofUnits(SI):TheModernMetricSystem33.Terminology3.1Definitions—The
10、terminologygiveninTerminologyD883isapplicabletothisspecificationunlessotherwisespecified.3.2DefinitionsofTermsSpecifictoThisStard:3.2.1bulkdensityn—themassinkilogramspercubicmetreofresincompoundmeasuredundertheconditions
11、ofthetest.3.2.2filledcompoundn—blendofPTFEresinasthematrixparticulatefillersgenerallyglassotheringanicmetallicpolymericmaterialsthatwithstthesinteringtemperatureofPTFE(327to380C).3.2.3freeflowresins(pelletized)n—generall
12、ymadebytreatmentoffinelydividedresinstoproducefreeflowingagglomerates.3.2.4lotn—oneproductionrun.3.2.5pigmentedcompoundn—acompoundinwhichapigmentisaddedfcolantpurposesonly.3.2.6stardflowresins(nonpelletized)n—finelydivid
13、edresinwithanaverageparticlesizelessthan100m.3.3Abbreviations—AbbreviationsareinaccdancewithTerminologyD1600.PTFEistheacronymfpolytetrafluoroethylene.4.Classification4.1ThisspecificationcoversthefollowingtwotypesofPTFEco
14、mpounds:4.1.1TypeI—Stardflowresins(nonpelletized)materialfgeneralpurposecompressionmolding.1ThisspecificationisunderthejurisdictionofASTMCommitteeD20onPlasticsisthedirectresponsibilityofSubcommitteeD20.15onThermoplasticM
15、aterials.CurrenteditionapprovedAug.12014.PublishedSeptember2014.iginallyapprovedin1991.Lastpreviouseditionapprovedin2012asD474511aε01.DOI:10.1520D474514.2FreferencedASTMstardsvisittheASTMwebsitewww.astm.gcontactASTMCusto
16、merServiceat.FAnnualBookofASTMStardsvolumeinfmationrefertothestard’sDocumentSummarypageontheASTMwebsite.3AvailablefromASTMInternationalHeadquarters100BarrHarbDriveWestConshohockenPA19428ASummaryofChangessectionappearsatt
17、heendofthisstardCopyright?ASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959.UnitedStates19.2.1TestBillet9.2.1.1Pritomoldingscreenthematerialthrougha2.0mmhsieveifnecessary.9.2.1.2Prefmsolidtestbilletsi
18、namold(seeFig.1)havingacrosssectionalareanotgreaterthan25.8cm2≤(4in.2)ofsufficientheighttocontainthesample.Endplugclearanceshallbesufficienttoensureescapeofentrappedairduringpressing.Amoldlengthof305to380mm(12to15in.)pro
19、ducesabilletapproximately50to75mm(2to3in.)long.Thebilletlengthshallnotexceed75mm(3in.).9.2.1.3Assemblethemold.Addtheresintothemold.thetopplugapplyhpressuremakingcertainthatthepusheriscenteredinthemold.Placethemoldinahydr
20、aulicpressremovethesupptringspacers.Increasetheloadingsmoothlytothefinalprefmingpressurein3to5min.Use20.7MPa(3000psi)fcompoundscontainingupto4%byweightfiller.Use34.5MPa(5000psi)fcompoundscontaining5to25%byweight68.9MPa(1
21、0000psi)fcompoundscontaining26%mefiller.Holdundermaximumpressuref2to5min.Openthepressremovethetoppusherfromthemoldfcetheprefmverticallyoutofthemoldusingacontinuoussmoothmovement.9.2.1.4Placetheprefminasinteringovensinter
22、inaccdancewiththeprocedureinTable4.9.2.1.5SectioningTestBillet:(1)Dividethetestbilletbyremovinga1.6mm(1?16in.)minimumfromoneendofthetestbilletpritopreparationofthetestspecimens.(2)Preparefivetestspecimens160.25mm(0.04060
23、.010in.)inthicknessfthedeterminationoftensilepropertiescutapieceofsuitablethicknessfspecificgravitymeasurements.Thispiecewillbeapproximatelycubicalinshapeweighingatleast10g.Allsurfacesmustbesmooth.Takecaretoavoidwedgesha
24、pecuts.9.2.2SpecificGravity(alternativemolding)9.2.2.1Pritomoldingscreenthematerialthrougha2.0mmhsieveifnecessary.9.2.2.2Acylindricalprefmingdie28.6mm(11?8in.)internaldiameterbyatleast76.2mm(3in.)deepthetestspecimenasagr
25、eedtoinX1.3isused.Endplugclearancesshallbesufficienttoensureescapeofairduringpressing.TABLE2TFECompoundsTypeIIFreeFlow(Pelletized)RawResinBulkDensitymingLMoldedParts(MoldedSintered)GradeSpecificGravityminSpecificGravitym
26、axTensileStrengthElongationmin%minMPaminpsi115%glassfiber6252.1502.2513.82000200225%glassfiber6252.1502.25012.41800150335%glassfiber6502.1502.2508.3120010045%glassfiber5%MoS25752.1502.30017.22500170515%glassfiber5%MoS260
27、02.1502.30013.81800120610%graphite6002.0702.19013.82000150715%graphite5502.1002.20010.3150060825%carbongraphite5001.9502.1008.3120020932%carbongraphite4001.9002.2006.91000201040%bronze7502.9503.25013.82000851160%bronze90
28、03.8004.00010.31500201255%bronze5%MoS29003.5004.0006.91000201350%stainlesssteel8503.2003.60013.820001000AsspecifiedbycustomersupplierAsspecifiedbycustomersupplier.TABLE3RequiredFillerContentMass%Tolerance%10to3124to25232
29、6to603461to755FIG.1PrefmingofPTFECompositeTestBilletTABLE4SinteringProceduresfTestBilletsInitialtemperatureC()AAmbientRateofheatingCh(Fh)605(1089)HoldtemperatureC(F)3706(69810)Holdtimemin2405RateofcoolingCh(Fh)605(1089)F
溫馨提示
- 1. 本站所有資源如無特殊說明,都需要本地電腦安裝OFFICE2007和PDF閱讀器。圖紙軟件為CAD,CAXA,PROE,UG,SolidWorks等.壓縮文件請下載最新的WinRAR軟件解壓。
- 2. 本站的文檔不包含任何第三方提供的附件圖紙等,如果需要附件,請聯(lián)系上傳者。文件的所有權(quán)益歸上傳用戶所有。
- 3. 本站RAR壓縮包中若帶圖紙,網(wǎng)頁內(nèi)容里面會有圖紙預(yù)覽,若沒有圖紙預(yù)覽就沒有圖紙。
- 4. 未經(jīng)權(quán)益所有人同意不得將文件中的內(nèi)容挪作商業(yè)或盈利用途。
- 5. 眾賞文庫僅提供信息存儲空間,僅對用戶上傳內(nèi)容的表現(xiàn)方式做保護(hù)處理,對用戶上傳分享的文檔內(nèi)容本身不做任何修改或編輯,并不能對任何下載內(nèi)容負(fù)責(zé)。
- 6. 下載文件中如有侵權(quán)或不適當(dāng)內(nèi)容,請與我們聯(lián)系,我們立即糾正。
- 7. 本站不保證下載資源的準(zhǔn)確性、安全性和完整性, 同時也不承擔(dān)用戶因使用這些下載資源對自己和他人造成任何形式的傷害或損失。
最新文檔
- 【astm標(biāo)準(zhǔn)】d 7976 - 14
- 【astm標(biāo)準(zhǔn)】d 4566 - 14
- 【astm標(biāo)準(zhǔn)】d 1518 - 14
- 【astm標(biāo)準(zhǔn)】d 7224 - 14
- 【astm標(biāo)準(zhǔn)】d 7400 - 14
- 【astm標(biāo)準(zhǔn)】d 6393 - 14
- 【astm標(biāo)準(zhǔn)】d 4772 - 14
- 【astm標(biāo)準(zhǔn)】d 5045 - 14
- 【astm標(biāo)準(zhǔn)】d 2274 - 14
- 【astm標(biāo)準(zhǔn)】d 1894 - 14
- 【astm標(biāo)準(zhǔn)】d 7268 - 14
- 【astm標(biāo)準(zhǔn)】d 1883 - 14
- 【astm標(biāo)準(zhǔn)】d 4417 - 14
- 【astm標(biāo)準(zhǔn)】d 7019 - 14
- 【astm標(biāo)準(zhǔn)】d 5195 - 14
- 【astm標(biāo)準(zhǔn)】d 5443 - 14
- 【astm標(biāo)準(zhǔn)】d 7396 - 14
- 【astm標(biāo)準(zhǔn)】d 5220 - 14
- 【astm標(biāo)準(zhǔn)】d 7668 - 14a
- 【astm標(biāo)準(zhǔn)】d 5147 - d 5147m - 14
評論
0/150
提交評論