稀土摻雜三偏磷酸鑭和焦磷酸鹽發(fā)光材料的制備與性能.pdf

1、學校代碼：10663學號：4201210000400貴州師范大學碩士學位論文稀土稀土摻雜摻雜三偏磷酸鑭和焦磷酸鹽三偏磷酸鑭和焦磷酸鹽發(fā)光材料發(fā)光材料的制備與性能的制備與性能SynthesispropertiesofrareearthdopedlanthanummetaphosphatepyrophosphatesM2P2O7(M=SrMgBa)phosphs專業(yè)名稱：分析化學專業(yè)代碼：070302研究方向：新型功能材料表征與分析申請人姓

2、名：賈曉卉導師姓名：楊錦瑜教授二零一五年五月三十日貴州師范大學碩士學位論文目錄i目錄目錄目錄................................................................................................................................i摘要摘要.........................................

3、.......................................................................................iABSTRACT...................................................................................................................i第一章第一章緒論

4、緒論.................................................................................................................11.1稀土與稀土離子..............................................................................................

5、11.1.1稀土概況................................................................................................11.1.2稀土離子................................................................................................11.2發(fā)光材料

6、發(fā)光及能量轉(zhuǎn)化過程......................................................................11.3稀土發(fā)光材料的應用......................................................................................21.4發(fā)光材料常見的合成方法...........................

7、...................................................21.4.1固相法....................................................................................................21.4.2沉淀法...................................................

8、.................................................21.4.3溶膠凝膠法..........................................................................................31.4.4水熱法.............................................................

9、.......................................31.5稀土多磷酸鹽研究進展..................................................................................31.5本論文的工作思路、主要內(nèi)容和創(chuàng)新點......................................................61.5.1工作思路

10、及目標....................................................................................61.5.2主要內(nèi)容................................................................................................61.5.3創(chuàng)新點..................

11、..................................................................................7第二章第二章樣品制備及分析測試品制備及分析測試.....................................................................................82.1實驗試劑.....................

12、.....................................................................................82.2實驗儀器..........................................................................................................92.3實驗過程.............

13、.............................................................................................92.3.1溶液配制................................................................................................92.3.2樣品制備過程.........

14、...............................................................................92.4分析測試........................................................................................................112.4.1熱重分析TGDTA.............

15、.................................................................112.4.2XRD分析.............................................................................................112.4.3粒度分析.......................................

16、.......................................................112.4.4FTIR分析............................................................................................112.4.5熒光光譜分析...............................................