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1、Designation:E1116?98(Reapproved2014)StardTestMethodfEmulsificationacteristicsofPesticideEmulsifiableConcentrates1ThisstardisissuedunderthefixeddesignationE1116thenumberimmediatelyfollowingthedesignationindicatestheyearof
2、iginaladoptioninthecaseofrevisiontheyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperepsilon()indicatesaneditialchangesincethelastrevisionreapproval.1.Scope1.1Thistestmethoddescribesageneralp
3、rocedurefthedeterminationofemulsificationspontaneitytheemulsionstabilityacteristicsofpesticideemulsifiableconcentrateswhendilutedwithwater.1.2Propersafetyhygieneprecautionsmustbetakenwhenwkingwithpesticidefmulationstopre
4、ventskineyecontactvapinhalationenvironmentalcontamination.Readfollowallhlinginstructionsfthespecificfmulationconductthetestinaccdancewithgoodlabatypractice.1.3ThevaluesstatedinSIunitsaretoberegardedasstard.Nootherunitsof
5、measurementareincludedinthisstard.1.4Thisstarddoesnotpurpttoaddressallofthesafetyconcernsifanyassociatedwithitsuse.Itistheresponsibilityoftheuserofthisstardtoestablishappropriatesafetyhealthpracticesdeterminetheapplicabi
6、lityofregulatylimitationspritouse.2.ReferencedDocuments2.1ASTMStards:2D1126TestMethodfHardnessinWaterD1193SpecificationfReagentWater3.Terminology3.1Definitions:3.1.1emulsificationspontaneity——therapidfmationofanemulsioni
7、nthetestwaterfromagitationprovidedonlybythegravityadditionoftheproduct.Fproductsofdensitygreaterthanthewaterusedanexcellentspontaneityratingisassignedwhentheemulsionbloom(billowing)extendsdownwardtonearthebottomofthewate
8、rwithnovisibleoilcreamletsreachingthebottomofthetestcylinder.Fproductsofdensitylessthanthewaterusedaratingofexcellentisgivenifbloomoccursnearthetopofthewaternofreeoilispresent.Spontaneitydeionsbetweenexcellentnil(noemuls
9、ionfmedonlyfreeoil)areassignedverygoodfairpoonasubjectivebasis.3.1.2emulsionquality—asubjectiveevaluationoftheemulsionappearance.Aratingofexcellent(homogeneous)verygoodgoodfairpo(nonhomogeneous)isassigned.3.1.2.1Discussi
10、on—Creamoilseparationmaycoexist.Nmallyoilislocatedateithertheextremetopbottomoftheliquidwithcreambetweenittherestoftheemulsion.Onrareoccasionsseparationoccursatbothtopbottomoftheliquid(becauseofpartitionsolubilitypropert
11、ies)caremustbetakentosonoterecd.3.2Separation:3.2.1separationcream—adiscreteopaquelayerofconcentratedemulsionoccurringateitherthetopthebottomoftheliquid.3.2.2separationoil—adiscretelayerofnonemulsifiedliquidoccurringatei
12、therthetopthebottomoftheliquid.4.SummaryofTestMethod4.1Inthistestmethodemulsifiablepesticideconcentratesareaddedtowaterofagivenhardnessataspecifiedtemperaturetofmanoilinwateremulsion.Perfmanceofthefmulationismeasuredinte
13、rmsofemulsionspontaneityemulsionstabilityunderstaticconditionsreemulsificationofthecoalescedphase.5.SignificanceUse5.1Thistestmethodprovidesaguidefevaluatingemulsificationacteristicsofpesticideemulsifiableconcentrates.It
14、definesthestabilityofemulsifiedparticlesinwater.Althoughnotabsolutethetestmethodisameasureofexpectedemulsionstabilityinagriculturalapplicationequipment.6.Apparatus6.1AnalyticalBalanceaccurateto0.01g.6.2Burets50100mLcapac
15、ity.1ThistestmethodisunderthejurisdictionofASTMCommitteeE35onPesticidesAntimicrobialsAlternativeControlAgentsisthedirectresponsibilityofSubcommitteeE35.22onPesticideFmulationsDeliverySystems.CurrenteditionapprovedOct.120
16、14.PublishedDecember2014.iginallyapprovedin1986.Lastpreviouseditionapprovedin2008asE1116–98(2008).DOI:10.1520E111698R14.2FreferencedASTMstardsvisittheASTMwebsitewww.astm.gcontactASTMCustomerServiceat.FAnnualBookofASTMSta
17、rdsvolumeinfmationrefertothestard’sDocumentSummarypageontheASTMwebsite.Copyright?ASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959.UnitedStates1ASTMInternationaltakesnopositionrespectingthevalidityofa
18、nypatentrightsassertedinconnectionwithanyitemmentionedinthisstard.Usersofthisstardareexpresslyadvisedthatdeterminationofthevalidityofanysuchpatentrightstheriskofinfringementofsuchrightsareentirelytheirownresponsibility.T
19、hisstardissubjecttorevisionatanytimebytheresponsibletechnicalcommitteemustbereviewedeveryfiveyearsifnotrevisedeitherreapprovedwithdrawn.Yourcommentsareinvitedeitherfrevisionofthisstardfadditionalstardsshouldbeaddressedto
20、ASTMInternationalHeadquarters.Yourcommentswillreceivecarefulconsiderationatameetingoftheresponsibletechnicalcommitteewhichyoumayattend.IfyoufeelthatyourcommentshavenotreceivedafairhearingyoushouldmakeyourviewsknowntotheA
21、STMCommitteeonStardsattheaddressshownbelow.ThisstardiscopyrightedbyASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959UnitedStates.Individualreprints(singlemultiplecopies)ofthisstardmaybeobtainedbyconta
22、ctingASTMattheaboveaddressat6108329585(phone)6108329555(fax)(email)throughtheASTMwebsite(www.astm.g).PermissionrightstophotocopythestardmayalsobesecuredfromtheCopyrightClearanceCenter222RosewoodDriveDanversMA01923Tel:(97
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