db51t 676-2007 牛奶中氯霉素殘留檢測(cè)方法-高效液相色譜-串聯(lián)質(zhì)譜(lc-ms-ms)法

1、ICS：65.020.30備案號(hào)：四川省地方標(biāo)準(zhǔn)DB51T676—2007牛奶中氯霉素殘留檢測(cè)方法－高效液相色譜串聯(lián)質(zhì)譜（LCMSMS）法Determinationofchlamphenicolresiduesinmilkbyhighperfmanceliquidchromatographytemmassspectrometry20070317發(fā)布20070501實(shí)施四川省質(zhì)量技術(shù)監(jiān)督局發(fā)布DBDBDB51T676—2007I目次前言.

2、..............................................................................II1范圍..................................................................................12規(guī)范性引用文件..............................................

3、..........................13制樣..................................................................................13.1樣品的制備..........................................................................13.2樣品的保存................

4、..........................................................14測(cè)定方法..............................................................................14.1方法提要或原理...................................................................

5、...14.2試劑和材料..........................................................................14.3儀器和設(shè)備..........................................................................24.4測(cè)定步驟...........................................

6、.................................24.5結(jié)果計(jì)算和表述......................................................................35檢測(cè)方法靈敏度、準(zhǔn)確度、精密度........................................................45.1靈敏度..........................

7、....................................................45.2準(zhǔn)確度..............................................................................45.3精密度............................................................................